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Reaction synthesis of bulk intermetallic materials from cold spray deposits from binary powders containing iron
Dyčková, Lucie ; Krajňáková, Petra (referee) ; Jan, Vít (advisor)
This thesis deals with reaction synthesis of materials Fe–Al, Fe–Cu and Fe–Ni from cold spray. In literature analysis are introduced these systems and for each system there is brief description of binary equilibrium diagram. Furthermore here are some short explanations of diffusion, Kirkendall effect and other possible processing technologies of intermetallic materials. In experimental part, samples of sprayed materials were annealed and then microstructural changes were investigated. This thesis contains photographs of microstructure, results from scanning electron microscopy, X-ray, and measurements of microhardness.
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Reaction synthesis of bulk Fe-Al intermetallic materials
Dyčková, Lucie ; Hutařová, Simona (referee) ; Jan, Vít (advisor)
Bachelor’s thesis deals with iron aluminides. In literature analysis are the best known and the most widely used intermetallics materials, diffusion and other possible processing technologies of intermetallic materials. In experimental part was used sprayed coating. This sprayed coating was produced by cold gas-dynamic spray. In this thesis were analysed changes in microstructure of iron aluminides depending on annealing temperature. This thesis contains photographs of microstructure and analyses from electron microscopy and measurement of microhardness.
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Reaction synthesis of bulk intermetallic materials from kinetic spraying deposits
Stejskal, Pavel ; Roupcová, Pavla (referee) ; Jan, Vít (advisor)
This work deals with issues of preparation of intermetallics based on iron, nickel and titanium aluminides. It works with an idea of preparation of bulk material by reaction synthe-sis from kinetic spraying deposits by cold spray. Theoretical part is concerned with phases and compounds of these aluminides for structural applications, their characteristics and present fabrication. In experimental part there are studied microstructures created by annealing of deposits.
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Nanoscale AFM and TEM observations of elementary dislocation mechanisms
Veselý, Jozef ; Cieslar, Miroslav (advisor) ; Dlouhý, Antonín (referee) ; Novák, Pavel (referee)
Single crystals of iron with 20, 28 and 40 at. % aluminium were deformed in compression at room temperature. The later two alloys were deformed also at temperatures in the range of yield stress anomaly. Room temperature deformation was carried under the atomic force microscope (AFM) and the evolution of surface was recorded in-situ. Samples deformed at elevated temperatures were investigated by AFM after the deformation. Dislocation structures in deformed samples were then investigated in transmission electron microscope (TEM). Observations of surface (AFM) and bulk (TEM) are compared. Results of both techniques mutually agree and support the interpretation of observed phenomena. Several original analysis methods were developed. Most notably the stereographic reconstruction, which was applied to dislocation structures and carbide particles present in investigated alloys. Model explaining the distribution of carbide particle axes is presented. Powered by TCPDF (www.tcpdf.org)
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Reaction synthesis of bulk intermetallic materials from cold spray deposits from binary powders containing iron
Dyčková, Lucie ; Krajňáková, Petra (referee) ; Jan, Vít (advisor)
This thesis deals with reaction synthesis of materials Fe–Al, Fe–Cu and Fe–Ni from cold spray. In literature analysis are introduced these systems and for each system there is brief description of binary equilibrium diagram. Furthermore here are some short explanations of diffusion, Kirkendall effect and other possible processing technologies of intermetallic materials. In experimental part, samples of sprayed materials were annealed and then microstructural changes were investigated. This thesis contains photographs of microstructure, results from scanning electron microscopy, X-ray, and measurements of microhardness.
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Reaction synthesis of bulk intermetallic materials from kinetic spraying deposits
Stejskal, Pavel ; Roupcová, Pavla (referee) ; Jan, Vít (advisor)
This work deals with issues of preparation of intermetallics based on iron, nickel and titanium aluminides. It works with an idea of preparation of bulk material by reaction synthe-sis from kinetic spraying deposits by cold spray. Theoretical part is concerned with phases and compounds of these aluminides for structural applications, their characteristics and present fabrication. In experimental part there are studied microstructures created by annealing of deposits.
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Reaction synthesis of bulk Fe-Al intermetallic materials
Dyčková, Lucie ; Hutařová, Simona (referee) ; Jan, Vít (advisor)
Bachelor’s thesis deals with iron aluminides. In literature analysis are the best known and the most widely used intermetallics materials, diffusion and other possible processing technologies of intermetallic materials. In experimental part was used sprayed coating. This sprayed coating was produced by cold gas-dynamic spray. In this thesis were analysed changes in microstructure of iron aluminides depending on annealing temperature. This thesis contains photographs of microstructure and analyses from electron microscopy and measurement of microhardness.
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